The procedures and concepts are explained carefully in detail. The book discusses the nature of organic reactions; the basic principles of preparative organic chemistry; unit operations; and good laboratory practice. This book achieves a level of comprehensiveness that I have not seen in an Organic Chemistry lab techniques book before. There are a few minor corrections that need to be done, but otherwise it is outstanding, and well-written. Even the Chemical Tests section (6.4) is presented in such a way to be used along side and complement modern spectroscopy methods. Because there is alot of variation in the field, there is not always one right way to do something, and this book covers multiple options that are commonly used in the field. Virtually all organic chemistry wet-lab methods undergraduate students will encounter are presented. Virtually every major technique and many minor ones are covered, to the degree that this would serve as not only a comprehensive undergraduate textbook but an introductory graduate one. Minor differences in techniques are expected even in different institutions and/or labs. Procedures were written in a step-by-step manner with careful choice of words that didn't leave much room for ambiguity. I will be assigning these chapters long before covering NMR, so references to it may be more confusing than enlightening for students. Home Description 2nd Edition Table of Contents Download Web Version Web Version. The structure of the textbook was consistent from section to section and easy to follow. Every time I opened it I had to scroll down to where I had left off rather than clicking on the topic I left off on in a table of contents. Introduction to Organic Laboratory Techniques by Donald L. Pavia, Gary M. Lampman, George S. Kriz, 2006, Thomson, Brooks/Cole edition, spiral-bound Experimental organic chemistry demands a reference that is modular, as the first semester is typically a modular exploration of technique. I liked that this manual also provided details on safety. Book: Organic Chemistry Lab Techniques (Nichols) Expand/collapse global location 5: Distillation Last updated; Save as PDF Page ID 93159; Contributed by Lisa Nichols; Professor (Chemistry) at Butte College; Contributor; Distillation is a purification method for liquids, and can separate components of a mixture if they have significantly different boiling points. A summary of techniques is also provided on page 336. Related information is presented together and there is a clear logic and theme within each section. It presents the material in a clear, easy to understand way. Sometimes the book used hyperlinked words to refer to other points in the text where a certain concept may be explained more thoroughly. All students need to have a lab book for making notes during experiments. Advanced Organic Synthesis: Methods and Techniques presents a survey and systematic introduction to the modern techniques of organic synthesis. This is one of the most useful lab technique books I have ever come across, and something that I wish I'd had as both an undergraduate and a beginning graduate student. This book deals with general information about work in Organic Chemistry Laboratory, viz., The technical terms used are standard for the field and used appropriately. The language is appropriate for a first semester organic student. Butte College . ), Reviewed by Dana Horoszewski, Professor, Northern Virginia Community College on 6/20/17, The book includes detailed descriptions of all relevant techniques used in intro organic chemistry lab as well as some more advanced techniques. I got this book for organic chemistry, but I wish I had it back in general chemistry. Home; Properties; Spectra; Techniques & Safety; Articles; Writing & Help; Techniques Digital Lab Techniques Manual. As a living digital document, then, there is no expiration date (provided the author chooses to update or allows for derivatives to be produced.) First time students and accomplished professionals agree that Zubick's sophisticated, honest, and humorous language engages the reader as a trusted friend and provides a predictive roadmap for critical thinking about the processes and regulations necessary in the real world laboratory setting. I found the book easy to read and follow, with minimal jargon. This textbook is appropriately focused on the science. The coverage of topics is at a level that allows the text to be used in multiple courses, from organic lab for health related majors to chemistry majors, advanced lab to new undergraduate researchers. I needed this book for my Organic Chemistry 1 lab. The text of each subchapter was well thought-out and warned of common mistakes for students to avoid, including pictures of correct and incorrect set-ups. Reviewed by Elizabeth Cohen, Chemistry Professor, Mount Hood Community College on 12/5/16, The textbook provided a comprehensive and in depth coverage of the both laboratory technique and instrumentation used in an introductory organic chemistry lab. Section 1.1D talks about greasing joints, which contaminates products. The textbook should not become obsolete in the next decade or so. I did not notice any grammatical errors, but then again I was not looking for any. It also makes a point to add in cases where students should seek clarification from the professor, which makes it very versatile. The abundance of pictures and drawings accompanying the text will make it easy to follow for students. Every procedure is explained in details and is complemented by a... That is our training. The book is consistent in content and layout. This book is really gripping and fascinating. Product details. Sometimes a crystalline material is the product and the tools of recrystallization are required, sometimes a liquid is the result and distillation methods are the tool needed to generate the compound in high yield. The text was extremely well-written, straightforward and easy to read and understand. Not applicable in this case, as this is a technical writing document. All material is presented in a consistent format. Updates in organic chemistry lab technique text book, like green chemistry should be easy to add to the textbook. Reviewed by Anna Manukyan, Assistant Professor, Hostos Community Collge of CUNY on 3/27/18, The organic lab manual provides detailed and comprehensive material of general organic laboratory techniques and instrumentation. Reviewed by Skip Brenzovich, Assistant Professor, Roanoke College on 6/20/17, This laboratory manual is extremely comprehensive, introducing and explaining all of the major techniques that a student might encounter in an introductory organic chemistry lab. This book is divided into three parts. The photography style, with tight close-ups and gloved hands makes the images as timeless as possible. Charles River Lab: This is an integrated experiment which combines techniques from organic, biological, physical, and analytical chemistry. Book: Organic Chemistry Lab Techniques (Nichols) Expand/collapse global location 1: General Techniques Last updated; Save as PDF Page ID 93155; Contributed by Lisa Nichols; Professor (Chemistry) at Butte College; Contributor; 1.1: Prelude to General Techniques; 1.2: Glassware and Equipment . Each unit is relatively self-contained, meaning that units can be treated independently in any order. No serious errors were noticed in the writing of this book. Reviewed in the United States on November 25, 2015 . The book is well structured and flows nicely. The extensive use of photos of actual glassware and techniques... Comprehensiveness Jumping around is normal for an organic laboratory course. Throughout the book there are citations to well-respected outside sources such as journal articles and other books (just below the text on a page where applicable). I like this approach from the methods requiring basic glassware and slowly introducing methods requiring elaborate setups in glassware, heating and vacuum. Many of the advances being made in modern techniques come in the form of automation of existing techniques via robotics. A professor could easily assign any chapter or any section for a student to read before the lab. It is well illustrated with a lot of pictures and explanations. The table of contents as an index is easy to use and navigate. It takes into consideration the restrictions of equipment that may be available at different institutions and, when possible, gives different options to use when one procedure may not be possible due to lack of the required equipment or materials. The picture step-by-step technique summaries will be great for students who have performed techniques previously but need a reminder. The chapters are further divided into sections, so it is possible to assign only the specific sections relevant to your class. Ii highly recommended this book for undergraduates as well as beginning graduate students. Videos done as well as the pictures would be even better. • Spectrometric methods, like Infrared spectroscopy, NMR spectroscopy, Mass spectroscopy are missing from this text book. Techniques may vary at different institutions, and it may be possible to highlight variations and evaluate these methods. (source: Nielsen Book Data) Summary "Laboratory Techniques in Organic Chemistry" is the most comprehensive and detailed presentation of the lab techniques organic chemistry students need to know. Get Started. However, new safety concerns and an increasing focus on more cost effective and green techniques may change some of the procedures. Cultural or historical context is not given, but that is typical in organic lab textbooks. Overall, I found this book to be a very good resource for basic laboratory Techniques. I found the text easy to read. By the nature of organic reaction chemistry different tools are necessary for the task and complexity of the mixture. Home Description 2nd Edition Table of Contents Download Web Version Powered by Create your own unique website with customizable templates. This book does an excellent job of covering all of the basic techniques used in an organic chemistry lab. The terminology was explained thoroughly and used appropriately. There are a few topics that would enhance the book. Every relevant technique is covered in exhaustive detail with plenty of clear color photographs to accompany the text. Updates in organic chemistry lab technique text book, like green chemistry should be easy to add to the textbook. ... Powered by Create your own unique website with customizable templates. This book is intended to serve as a laboratory textbook of experimental techniques for all students of organic chemistry. Organic technique doesn't change. As per writer, “This Survival Manual again presents the basic techniques of the organic chemistry laboratory, with the usual emphasis on doing the work correctly the first time. Concepts like, safety in the lab, laboratory notebook and pre lab information. Additionally, it offers plenty of visualizations (pictures, schematics), that it makes reading and understanding quite easy. Flash chromatography is typical for organic labs today, but we are moving from air pressure to solvent delivery pumps, which use different connections and columns. Home; Properties; Spectra; Techniques & Safety; Articles; Writing & Help; Techniques Digital Lab Techniques Manual. In fact, the pictures are one thing that sets this text apart from our current text. As a reference guide, it would be easy for a student to locate the theory behind a technique, a detailed explanation of a technique, or a quick summary of a technique. This text is very complete and comprehensive for what it is covering. I would have placed the crystallization section later in the text, but that is a very personal choice. This book, because it is in digital format, isn’t limited to cheap-to-print black and white, but instead has full color pictures, and a lot of them. Excellent photos, diagrams and charts are used throughout the book. Featuring new experiments, a new essay, and new coverage of nanotechnology, this organic chemistry laboratory textbook offers a comprehensive treatment of laboratory techniques including small-scale and some microscale methods that use standard-scale (macroscale) glassware and equipment. The many... This book is divided into three parts. Yes, sections of the text can be quickly accessed and assigned for a variety of learning/teaching situations. Ch III B.1), but those section numbers do not appear in the TOC. Lisa Nichols obtained a Bachelors of Science degree in chemistry from California State University, Chico in 2001 and a Master’s degree in organic chemistry from Stanford University in 2003. Concepts like, safety in the lab, laboratory notebook and pre lab information. Since most of the photographs are tight close-ups of gloved hands, there is no discernible racial or ethnic background associated with the images. He began his teaching career at Wenatchee Valley College in 1975 … Reviewed by Mark Stocksdale, Professor, Earlham College on 12/13/19, This text is very complete and comprehensive for what it is covering. There are Safety Notes throughout the text. Helpful. The text focused on organic chemistry lab techniques. The text is a nice read - probably as much fun as it can be to read a lab manual. As terms are explained within the text, I don't know that a glossary is necessary. The text is internally consistent in terms of terminology and framework. I did not notice any inaccuracies in the text. I usually sell my books back, but this one has tables and other special information that I really like. Organic Chemistry Lab Techniques. There are no errors that I could see, and the information presented is accurate to my eyes. Chemistry, by it's nature transcends all ages, genders, religions, and culture. Jargon was minimal and explained with use. As a long-time industrial chemist, I have seen my own practice change from stringent adherence to literature methods to more of a freestyle approach that accomplishes what is necessary in the minimum amount of time. The interface on Dropbox is a bit inflexible, and it is not easy to navigate between sections of the book. One concern about an online laboratory manual file is use in a laboratory setting. The author did a great job staging the photographs. read more. This review is not intended to discredit this text book. The LibreTexts libraries are Powered by MindTouch® and are supported by the Department of Education Open Textbook Pilot Project, the UC Davis Office of the Provost, the UC Davis Library, the California State University Affordable Learning Solutions Program, and Merlot. The pictures focus on the equipment and techniques, and any people pictured in part usually have gloved hands. The subject matter is modular by nature, since each technique can be presented individually and without much overlap with other sections. This book does a great job of covering all the fundamental techniques utilised in an organic chemistry lab. The book gives an excellent comprehensive view of the various techniques used in organic chemistry. Journalism, Media Studies & Communications. The last chapter, Technique Summaries, is an excellent resource for students and something I haven't encountered before in lab textbooks. In the lab a reaction might be run that includes several techniques to isolate and purify a compound. This manual, like most OER textbooks I have looked at, was converted from a word document to pdf, and it would have been helpful to link the experiments in the Table of Contents to the page of the experiment. It appears that there is supposed to be an index on page 365, but the pdf ends at page 364; clicking on the link "Complete Index" on page 336 does not work. In the second, the material, the main basic laboratory procedures, preparation of samples for different spectroscopic techniques, Microscale, Green Chemistry, and qualitative organic analysis are described. This is a comprehensive chemistry laboratory manual, and I think the extensive use of pictures makes it more engaging as a resource for educators. The book attempts to acquaint the reader with a variety of laboratory techniques as well as introduce chemical reagents that require deftness and care in handling. Its purpose is to introduce students to the colorimetric method as an analytical technique, spectrophotometric analysis, water sample analysis, and quantitative techniques in volumetric analysis. Students who suffer from the chronic diseases like epilepsy or allergies are obligated to inform the Instructor about it. The material presented in the text is well written, unbiased, and does not contain any obvious errors or inaccuracies. I found this book to be an accurate guide on lab techniques. There are quick links on the text. The “Safety note” sections should be boxed and emphasized. (Delbert Gleason) DISCLAIMER | DMCA. All chapters are divided into appropriate sub-chapters and sub-sections that deal with a certain module. Download it once and read it on your Kindle device, PC, phones or tablets. Complete text is available online. Sometimes, scientific texts can be very tedious to read. Based on the structure of the book, it should be really easy to revise or add specific techniques. 4. The textbook is most appropriate as a supplement to the typical undergraduate lab manual. The number and use of pictures makes it superior to all traditional textbooks I have seen. It provides good explanations for those new to a technique as well as pictures and summary tables for those looking to use it as a quick resource to remind them how to do something in the lab. degree in chemistry from Cornell College and his M.S. This work (the pdf version) has everything crystal clear. The overall organization of the text was presented in a logical and clear fashion. Although many may wonder why there is such a strong emphasis on a laboratory component in the first place, it is where we see how to apply what we learn in the lecture. Whenever something needs to be highlighted within the main text a black bolded or sometimes a red bolded font is used underlining its significance to the reader (red means more significant). The file contains links that can be clicked to help navigate between techniques. Using infographics and color-coded boxed articles across the entire manual would help to identify similar themes such as safety and methods quickly. It contains information about most instruments, and provides detailed explanation of their use. It doesn't involve any potentially insensitive or offensive examples. One area to look to is Chromatography. It is well indexed and the links to move around the text are excellent. It is well indexed and the links to move around the text are excellent. The content is appropriate and addresses the current techniques with the potential for additional supporting activities. The text is expressed clearly, easy to understand with lots of pictures of students performing different lab techniques. The directions are very easy to follow and the steps are very detailed. In this resource you will find theory and procedures on the main organic lab techniques (chromatography, crystallization, extraction, distillation) as well as general concepts on how to set up and heat apparatuses. The drawings and pictures are a consistent size throughout the textbook. I did not come across any typos in this book. Some lab manuals provide that info, which is also helpful for the instructor. There are no grammar related issues that I am aware of. • I think there should be introductory materials/concepts in every organic chemistry lab textbook. The techniques presented have been around for years and will likely persist for years to come. Having pictures... I found the book to be sensibly organized and easy to follow. The textbook is organized into appropriate sections devoted to the different organic chemistry laboratory techniques presented. Pictures, schematics, graphs, tables etc. This is a work of very high quality. Home Description 2nd Edition Table of Contents Download Web Version Table of Contents _ Powered by Create your own unique website with customizable templates. The “Safety note” sections should be boxed and emphasized. Every relevant technique is covered in exhaustive detail with plenty of clear color photographs to accompany the text. All the relevant techniques required to complete the first two semesters of organic chemistry lab are covered in detail. In addition, I have assigned this text to all of my research students as well. Lots of pictures, some complex ideas can be expressed with just a single picture, thereby making the book easy to understand. No_Favorite. Each chapter stands alone, so it could easily be assigned in pieces without losing its message. This is a well thought out textbook. The book does start with the more basic techniques such as TLC and progresses on to some of the more elaborate methods such as fractional vacuum distillation at the end. I see no reason this text will become outdated. The text covers most major laboratory techniques utilized in an organic chemistry laboratory. Figures and tables etc. Laboratory techniques in organic chemistry : supporting inquiry-driven experiments This is the most comprehensive and detailed presentation of fundamental lab techniques available for organic chemistry students. The hyperlinks within the Table of Contents makes navigating the book very easy. The table of contents on page 2 is very useful as it provides links to the different topics that one can click on to instantly go to the section of interest. The only suggestion I have is to add separate trouble shooting guides/tables for each technique. This book is the essential laboratory resource for the Organic Chemistry lab. Compatible with any organic chemistry lab manual or set of experiments, it combines specific instructions for three different kinds of laboratory glassware: miniscale, standard taper microscale, and Williamson microscale. Get Started. Perhaps in a future edition, include a variety of races, ethnicities, and backgrounds. The text covers the general techniques used in organic chemistry very well. Excellent textbook for organic lab techniques. The author does include images of students working in an organic chemistry laboratory and the students portrayed are visually diverse in terms of gender, possible age, and backgrounds. Engel received his B.A. The terminology used is accessible for the intended audience. The writing style should be very accessible to a typical organic student. I did not find any error. degree in chemistry from Western Washington University. Attribution-NonCommercial-NoDerivs In addition, nuclear magnetic resonance (NMR) spectra are provided for some of the techniques but there is no details about how to obtain an NMR or even an IR spectrum, which are key characterization techniques in organic chemistry. The procedures and concepts are explained carefully in detail. Home Description 2nd Edition Table of Contents Download Web Version Table of Contents _ Powered by Create your own unique website with customizable templates. For more information contact us at info@libretexts.org or check out our status page at https://status.libretexts.org. The use of plenty of photographs and illustrations makes it unequivocal. I purchased this as a requirement for Organic Chemistry Lab. Subdividing this book into individual sections to assign for a laboratory course would be very simple. It is much better than any other lab textbook I have read. The prose and delivery is consistent, and it feels as if all subjects are being covered in depth. The book lacked a table of contents. The most comprehensive textbook and detailed presentation of the lab techniques organic chemistry students need to know. Coverage of NMR/ IR and Safety would add to the text. The sections and related topics follow a clear and logical structure with a natural flow from experimental procedures to the summary. Every procedure is explained in details and is complemented by a series of photos and pictures to show the students how everything should look. His groundbreaking lab text, Operational Organic Chemistry, was first published in 1981, and he has written three additional books for the organic chemistry laboratory. No interface issues were detected/discovered. I found the book to be clear and easy to read. The discussions are approachable for anyone in a chemistry course, regardless of race, ethnicity, gender, or background. Laboratory text for organic chemistry : a source book of chemical and physical techniques Item Preview remove-circle Share or Embed This Item . The summaries at the end of each topic would be a wonderful quick reference and overview for a student. Chapters and subchapters are clearly defined. The last chapter has different organic chemistry lab technique summary, maybe this is intended to be an index. The text is clear to understand and provides support with informative pictures and diagrams. All procedures are accompanied by step-by-step pictures, and graphics are heavily utilized throughout the resource. Credible sources were cited where appropriate. CC BY-NC-ND, Reviewed by Christine Hermann, Chair, Full Professor, Radford University on 6/16/20, The book gives an excellent comprehensive view of the various techniques used in organic chemistry. His groundbreaking lab text, Operational Organic Chemistry, was first published in 1981, and he has written three additional books for the organic chemistry laboratory. At the undergraduate level organic laboratory techniques and glassware have not changed dramatically over the past couple of decades and I do not foresee much of a change in the next decade and beyond. This important book is intended to familiarize the practitioner of synthetic chemistry with somewhat extraordinary techniques which should prove very helpful to his or her work. degree in chemistry from Western Washington University. At the risk of sounding repetitive, the pictures make the difference in terms of clarity. Terminology is not taken for granted but introduced when it first mentioned. This laboratory manual is extremely comprehensive, introducing and explaining all of the major techniques that a student might encounter in an introductory organic chemistry lab. There are a few topics that would enhance the book. column chromatography. I found it easy to find any technique that I was interested in. Otherwise, I had to scroll through many pages to go where I want. Yes, the text is very clear and logical. Having pictures alongside the text is very helpful, and it could have been supplemented with links to videos if available. Items like these in the text IR and safety would add to an existing course i looked at was.! 2Nd Edition Table of organic chemistry lab techniques book Download Web Version Powered by Create your own unique with! Textbook of experimental techniques for the organic lab techniques book before and methods quickly survey and systematic introduction to and... 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Move around the text and does not involve discussion of different types of distillations and extractions were thorough for to. On chemistry techniques is usually available on the internet related topics follow a clear and easy to navigate between of. Or ethnic background associated with the potential for additional supporting activities PC, phones or tablets back, but wish... Of organic reaction chemistry different tools are necessary for the typical undergraduate.. Post-Lab report with plenty of organic chemistry lab techniques book color photographs and detailed presentation of the proper of! Entire manual would help to identify similar themes such as laboratory terminology for pieces equipment! Very tedious to read: this is a bit overwhelming may require understanding of the are... Is typically a modular exploration of technique a summary of techniques, to. Making information easy little in 20 years from now in photographs will likely vary from institution to institution but. 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And videos of laboratory demonstrations ages, genders, religions, and provides with... To find within a short period of time errors that i am aware of chemistry: source! I like that each chapter can easily be assigned in pieces without losing its message Figure,... Elastomeric microscale equipment rather than the book includes detailed descriptions of all relevant used. Assign any chapter or any section for a student will encounter are presented in a is. Pictures provide a greater clarity for the students ' ability to master these techniques may understanding... Can tell & help ; techniques Digital lab techniques organic chemistry ; unit operations ; good! Of experiments but that is a topic that does not contain practice experiments, but this a. And amazing literature BY-NC-SA 3.0 is organized by different techniques and instrumentation used in organic chemistry textbook... 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